Technology Process of C21H29NO
There total 3 articles about C21H29NO which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium(II) trifluoroacetate; caesium carbonate; tricyclohexylphosphine;
In
para-xylene;
Inert atmosphere;
Reflux;
DOI:10.1002/cphc.201201069
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -30 °C
1.2: 2 h / 20 °C
2.1: caesium carbonate; palladium(II) trifluoroacetate; tricyclohexylphosphine / para-xylene / Inert atmosphere; Reflux
With
n-butyllithium; palladium(II) trifluoroacetate; caesium carbonate; tricyclohexylphosphine;
In
tetrahydrofuran; hexane; para-xylene;
DOI:10.1002/cphc.201201069
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / mineral oil; tetrahydrofuran / 1.17 h / 0 °C / Inert atmosphere
1.2: 19 h / 20 °C / Inert atmosphere; Reflux
2.1: caesium carbonate; palladium(II) trifluoroacetate; tricyclohexylphosphine / para-xylene / Inert atmosphere; Reflux
With
palladium(II) trifluoroacetate; sodium hydride; caesium carbonate; tricyclohexylphosphine;
In
tetrahydrofuran; para-xylene; mineral oil;
DOI:10.1002/cphc.201201069