SDZ 282396

Base Information Edit

Chemical Name:SDZ 282396
CAS No.:161510-35-6
Molecular Formula:C₃₅H₄₆N₄O₅
Molecular Weight:602.774
Hs Code.:
Mol file:161510-35-6.mol

Synonyms:SDZ 282396

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Chemical Property of SDZ 282396 Edit

Chemical Property:

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Technology Process of SDZ 282396

There total 6 articles about SDZ 282396 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 106566-02-3,120369-25-7,144902-31-8
L-valine benzylamide

: 161510-68-5
(2R,3S,4S)-2-(benzylamino)-4-<<(1,1-dimethylethoxy)carbonyl>amino>-3-hydoxy-5-phenylpentanoic acid

: 161510-35-6
SDZ 282396

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1021/jm00045a013

Reference yield:

: 124818-94-6,116246-06-1
ethyl (2E,4S)-4-[(tert-butoxycarbonyl)amino]-5-phenylpent-2-enoate

: 161510-35-6
SDZ 282396

Guidance literature:: Multi-step reaction with 4 steps

1: 62 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 120 h / Ambient temperature

2: 83 percent / ethanol / 48 h / 60 °C

3: 92 percent / 1N aq. NaOH / tetrahydrofuran / 10 h / Ambient temperature

4: 63 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide / dimethylformamide / 24 h / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00045a013

Reference yield:

: 72155-45-4
Boc-L-phenylalaninal

: 161510-35-6
SDZ 282396

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / toluene / 1 h / 80 °C

2: 62 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 120 h / Ambient temperature

3: 83 percent / ethanol / 48 h / 60 °C

4: 92 percent / 1N aq. NaOH / tetrahydrofuran / 10 h / Ambient temperature

5: 63 percent / 1-hydroxybenzotriazole, N,N'-dicyclohexylcarbodiimide / dimethylformamide / 24 h / Ambient temperature

With sodium hydroxide; benzotriazol-1-ol; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00045a013