1,3-bis[fluoro(dimethyl)silyl]-2,2,4,4-tetra(propan-2-yl)-1,3,2,4-diazadisiletidine

Base Information

• Chemical Name: 1,3-bis[fluoro(dimethyl)silyl]-2,2,4,4-tetra(propan-2-yl)-1,3,2,4-diazadisiletidine
• CAS No.: 83312-37-2
• Molecular Formula: C₁₆H₄₀F₂N₂Si₄
• Molecular Weight: 410.846
• Mol file: 83312-37-2.mol

Synonyms:NSC369735

Chemical Property of 1,3-bis[fluoro(dimethyl)silyl]-2,2,4,4-tetra(propan-2-yl)-1,3,2,4-diazadisiletidine

Chemical Property:

• Vapor Pressure: 0.00022mmHg at 25°C
• Boiling Point: 326.2°Cat760mmHg
• Flash Point: 151.1°C
• Density: 0.93g/cm³

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-bis[fluoro(dimethyl)silyl]-2,2,4,4-tetra(propan-2-yl)-1,3,2,4-diazadisiletidine

There total 3 articles about 1,3-bis[fluoro(dimethyl)silyl]-2,2,4,4-tetra(propan-2-yl)-1,3,2,4-diazadisiletidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

difluorodiisopropylsilane (426-05-1) → 1,3-Bis-(fluoro-dimethyl-silanyl)-2,2,4,4-tetraisopropyl-[1,3,2,4]diazadisiletidine (83312-37-2)

Guidance literature:

Multi-step reaction with 3 steps

1: LiNH₂

2: 1.) BuLi

3: 1.) BuLi

With n-butyllithium; lithium amide;

Reference yield:

(Fluor)diisopropylsilylamin (83312-31-6) → 1,3-Bis-(fluoro-dimethyl-silanyl)-2,2,4,4-tetraisopropyl-[1,3,2,4]diazadisiletidine (83312-37-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) BuLi

2: 1.) BuLi

With n-butyllithium;

Reference yield:

dimethyldifluorosilane (353-66-2) + 2,2,4,4-Tetraisopropylcyclodisilazan (83312-34-9) → 1-(Fluoro-dimethyl-silanyl)-2,2,4,4-tetraisopropyl-[1,3,2,4]diazadisiletidine (83312-36-1) + 1,3-Bis-(fluoro-dimethyl-silanyl)-2,2,4,4-tetraisopropyl-[1,3,2,4]diazadisiletidine (83312-37-2)

Guidance literature:

With n-butyllithium; Multistep reaction;

upstream raw materials:

dimethyldifluorosilane

2,2,4,4-Tetraisopropylcyclodisilazan

difluorodiisopropylsilane

(Fluor)diisopropylsilylamin

Refernces