triethylbenzylammonium 2,4-dinitrophenoxide

Base Information

• Chemical Name: triethylbenzylammonium 2,4-dinitrophenoxide
• CAS No.: 138554-42-4
• Molecular Formula: C₆H₃N₂O₅*C₁₃H₂₂N
• Molecular Weight: 375.425
• Mol file: 138554-42-4.mol

Synonyms:triethylbenzylammonium 2,4-dinitrophenoxide

Chemical Property of triethylbenzylammonium 2,4-dinitrophenoxide

Chemical Property:

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Technology Process of triethylbenzylammonium 2,4-dinitrophenoxide

There total 1 articles about triethylbenzylammonium 2,4-dinitrophenoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyl-N,N,N-triethylammonium chloride (56-37-1) + 2,2,4,4,6-Pentachloro-6-(2,4-dinitro-phenoxy)-2λ5,4λ5,6λ5-[1,3,5,2,4,6]triazatriphosphinine (157033-41-5) → triethylbenzylammonium 2,4-dinitrophenoxide (138554-42-4)

Guidance literature:

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; 4-nitro-phenol; buffer pH 9.18; In chlorobenzene; at 24.9 ℃; Equilibrium constant;

Reference yield: 98.0%

triethylbenzylammonium 2,4-dinitrophenoxide (138554-42-4) → 2,4-dinitrophenoxypentachlorocyclophosphazene

Guidance literature:

With 2,2,4,4,6,6-hexachloro-1,3,5-triaza-2,4,6-triphosphorine; In chlorobenzene; at 298 ℃; reactivity of salts of nitrophenols in the phenolysis of phosphazenes; other nitrophenols, phosphazenes and solvents;

Reference yield: 96.0%

1,5,1'',5''-tetrahydro-6',6'-(Cl2)-(1,2-(C2)-closo-dodecaborano(12){1,2-e}-1,3,2-dioxaphosphepin)-3-spiro-2'-(1,3,5,2.lamba.5,4λ5,6λ5-triazatriphosphorine)-4'-spiro-3''-(1,2-dicarba-closo-dodecacarborano-(12)){1,2-e}-1,3,2-dioxaphosphepin (110839-10-6) + triethylbenzylammonium 2,4-dinitrophenoxide (138554-42-4) → P3N3ClO(2,4-dinitrophenolate)((OCH2)2B10C2H10)2

Guidance literature:

In chlorobenzene; byproducts: (C2H5)3NCH2C6H5Cl; phenolysis at 298-328 K; irreversible reaction; mechanism discussed;; chromy. (silica gel/benzene);; Kinetics;

upstream raw materials:

N-benzyl-N,N,N-triethylammonium chloride

2,2,4,4,6-Pentachloro-6-(2,4-dinitro-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Downstream raw materials:

N-benzyl-N,N,N-triethylammonium chloride

2,2,4,4,6-Pentachloro-6-(2,4-dinitro-phenoxy)-2λ⁵,4λ⁵,6λ⁵-[1,3,5,2,4,6]triazatriphosphinine

Refernces