phenaceturic acid α-phenethylamide

Base Information

• Chemical Name: phenaceturic acid α-phenethylamide
• CAS No.: 102016-26-2
• Molecular Formula: C₁₈H₂₀N₂O₂
• Molecular Weight: 296.369
• Mol file: 102016-26-2.mol

Synonyms:phenaceturic acid α-phenethylamide

Chemical Property of phenaceturic acid α-phenethylamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of phenaceturic acid α-phenethylamide

There total 9 articles about phenaceturic acid α-phenethylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

benzylpenicilloic acid α-phenylethylamide (121766-89-0) → benzoimidazole (51-17-2,79351-71-6) + 3,3-dimethyl-D-cysteine (52-67-5) + phenaceturic acid α-phenethylamide (102016-26-2)

Guidance literature:

With 1,2-diamino-benzene; In water; acetic acid; for 1.5h; Heating;

DOI:10.1248/cpb.36.1957

Reference yield: 91.0%

benzylpenicilloic acid α-phenylethylamide (121766-89-0) + 1,2-diamino-benzene (95-54-5) → benzoimidazole (51-17-2,79351-71-6) + 3,3-dimethyl-D-cysteine (52-67-5) + phenaceturic acid α-phenethylamide (102016-26-2)

Guidance literature:

In water; acetic acid; for 1.5h; Heating;

DOI:10.1248/cpb.36.1957

Reference yield: 88.0%

N-phenethyl-α-phenylacetamido-2-benzothiazolidineacetamide (121766-91-4,121842-57-7) → 1,3-Benzothiazole (95-16-9) + phenaceturic acid α-phenethylamide (102016-26-2)

Guidance literature:

With toluene-4-sulfonic acid; In ethanol; for 3h;

DOI:10.1248/cpb.36.1957

upstream raw materials:

N-phenethyl-α-phenylacetamido-2-benzothiazolidineacetamide

benzylpenicilloic acid α-phenylethylamide

1,2-diamino-benzene

naphthalene-1,8-diamine

Refernces

• 1、 Ogawa, Toshihisa,Tomisawa, Kazuyuki,Sota, Kaoru. "PREPARATION OF D-PENICILLAMINE. REACTION OF PENILLOIC ACID, PENICILLOIC ACID α-AMIDES AND BENZYLPENICILLIN WITH N,N'-DIPHENYLETHYLENEDIAMINE". . p. 2815 - 2824. Retrieved 2007/10/02.