3-Nitropropanaldiethylacetal

Base Information

• Chemical Name: 3-Nitropropanaldiethylacetal
• CAS No.: 107833-73-8
• Molecular Formula: C7H15 N O4
• Molecular Weight: 177.2
• Hs Code.: 2911000000
• Mol file: 107833-73-8.mol

Synonyms:3-Nitropropanaldiethylacetal

Chemical Property of 3-Nitropropanaldiethylacetal

Chemical Property:

• PSA: 64.28000
• LogP: 1.57550

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Nitropropanaldiethylacetal

There total 1 articles about 3-Nitropropanaldiethylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

3-nitropropionaldehyde (58657-26-4) + orthoformic acid triethyl ester (122-51-0) → 3-nitropropanal diethyl acetal (107833-73-8)

Guidance literature:

toluene-4-sulfonic acid; In methanol; for 16h; Ambient temperature;

Reference yield: 98.0%

3-nitropropanal diethyl acetal (107833-73-8) → aminopropane diethyl acetal (41365-75-7)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 12h; under 7600.51 Torr;

DOI:10.1016/j.tetasy.2012.12.009

Reference yield:

3-nitropropanal diethyl acetal (107833-73-8) + 1-[(4-methoxyphenyl)methyl]piperidin-4-one (905986-94-9) → C18H28N2O6

Guidance literature:

With potassium hydroxide; In methanol; water; at 0 - 20 ℃; for 4h;

upstream raw materials:

3-nitropropionaldehyde

orthoformic acid triethyl ester

Downstream raw materials:

aminopropane diethyl acetal

Refernces

• 1、 Griesser,?hrlein,Schwab,Ehrler,J?ger,Davidson, James P.,Martin, Stephen F.. "3-Nitropropanal, 3-Nitropropanol, and 3-Nitropropanal dimethyl acetal [ Propanal, 3-nitro-; 1-Propanol, 3-nitro-; and Propane, 1,1-dimethoxy-3-nitro-]". . p. 236 - 236. Retrieved 2017/10/06.