2,3-DIHYDRO-6-ISOTHIOCYANATO-1,4-PHTHALAZINEDIONE

Base Information

• Chemical Name: 2,3-DIHYDRO-6-ISOTHIOCYANATO-1,4-PHTHALAZINEDIONE
• CAS No.: 107807-39-6
• Molecular Formula: C₉H₅N₃O₂S
• Molecular Weight: 219.224
• Hs Code.: 29339900
• Mol file: 107807-39-6.mol

Synonyms:Isoluminol isothiocyanate;1,4-Phthalazinedione,2,3-dihydro-6-isothiocyanato- (9CI);4-Isothiocyanatophthalhydrazide;

Chemical Property of 2,3-DIHYDRO-6-ISOTHIOCYANATO-1,4-PHTHALAZINEDIONE

Chemical Property:

• Melting Point: 41 °C
• Refractive Index: 1.767
• PKA: 9.91±0.20(Predicted)
• PSA: 110.17000
• Density: 1.59 g/cm³
• LogP: 0.95070
• Storage Temp.: Refrigerator

Purity/Quality:

99% ^*data from raw suppliers

2,3-Dihydro-6-isothiocyanato-1,4-phthalazinedione 96% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DIHYDRO-6-ISOTHIOCYANATO-1,4-PHTHALAZINEDIONE

There total 1 articles about 2,3-DIHYDRO-6-ISOTHIOCYANATO-1,4-PHTHALAZINEDIONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

thiophosgene (463-71-8) + isoluminol (3682-14-2) → isoluminol isothiocyanate (107807-39-6)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1246/cl.2011.188

upstream raw materials:

thiophosgene

isoluminol

Refernces