C₃₁H₃₁NO₃

Base Information

• Chemical Name: C₃₁H₃₁NO₃
• CAS No.: 1470017-26-5
• Molecular Formula: C₃₁H₃₁NO₃
• Molecular Weight: 465.592
• Mol file: 1470017-26-5.mol

Synonyms:C₃₁H₃₁NO₃

Chemical Property of C₃₁H₃₁NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₁H₃₁NO₃

There total 6 articles about C₃₁H₃₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3,4-dibenzyloxyphenylethyl)-β-(3'-methoxyphenyl)acetamide (1470017-24-3) → C31H31NO3 (1470017-26-5)

Guidance literature:

N-(3,4-dibenzyloxyphenylethyl)-β-(3'-methoxyphenyl)acetamide; With phosphorus pentoxide; trichlorophosphate; In toluene; at 0 ℃; for 6h; Inert atmosphere; Reflux;

With sodium tetrahydroborate; In methanol; at -78 ℃; for 2h; Inert atmosphere; Reflux;

DOI:10.1016/j.ejmech.2013.07.036

Reference yield:

3,4-dibenzyloxybenzaldehyde (5447-02-9) → C31H31NO3 (1470017-26-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: acetic acid; ammonium acetate / 4 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / Inert atmosphere; Reflux

3.1: sodium hydroxide / dichloromethane; water / 3 h / 0 - 20 °C

4.1: phosphorus pentoxide; trichlorophosphate / toluene / 6 h / 0 °C / Inert atmosphere; Reflux

4.2: 2 h / -78 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; phosphorus pentoxide; ammonium acetate; acetic acid; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; 3.1: |Schotten-Baumann Reaction / 4.1: |Bischler-Napieralski Reaction;

DOI:10.1016/j.ejmech.2013.07.036

Reference yield:

3,4-bis(benzyloxy)-β-nitrostyrene (1699-54-3) → C31H31NO3 (1470017-26-5)

Guidance literature:

Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 2 h / Inert atmosphere; Reflux

2.1: sodium hydroxide / dichloromethane; water / 3 h / 0 - 20 °C

3.1: phosphorus pentoxide; trichlorophosphate / toluene / 6 h / 0 °C / Inert atmosphere; Reflux

3.2: 2 h / -78 °C / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; phosphorus pentoxide; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; 2.1: |Schotten-Baumann Reaction / 3.1: |Bischler-Napieralski Reaction;

DOI:10.1016/j.ejmech.2013.07.036

upstream raw materials:

3,4-dibenzyloxybenzaldehyde

3,4-bis(benzyloxy)-β-nitrostyrene

3,4-di(benzyloxy)phenethylamine

N-(3,4-dibenzyloxyphenylethyl)-β-(3'-methoxyphenyl)acetamide

Refernces