docosyl 4-methylbenzoate

Base Information

• Chemical Name: docosyl 4-methylbenzoate
• CAS No.: 1036648-35-7
• Molecular Formula: C₃₀H₅₂O₂
• Molecular Weight: 444.742
• Mol file: 1036648-35-7.mol

Synonyms:docosyl 4-methylbenzoate

Chemical Property of docosyl 4-methylbenzoate

Chemical Property:

Purity/Quality:

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Technology Process of docosyl 4-methylbenzoate

There total 1 articles about docosyl 4-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-docosanol (661-19-8) + 4-methyl-benzoyl chloride (874-60-2) → docosyl 4-methylbenzoate (1036648-35-7)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; In dichloromethane; at -78 ℃; for 0.5h;

DOI:10.1039/b813545b

Reference yield: 63.0%

docosyl 4-methylbenzoate (1036648-35-7) → n-docosane (629-97-0)

Guidance literature:

docosyl 4-methylbenzoate; With samarium diiodide; In Norlaudanosolin; Inert atmosphere; Reflux;

With water; ammonium chloride; In Norlaudanosolin; Inert atmosphere;

DOI:10.1021/ol800944p

upstream raw materials:

1-docosanol

4-methyl-benzoyl chloride

Downstream raw materials:

n-docosane

Refernces

• 1、 Lam, Kevin,Markó, István E.. "Toluates: unexpectedly versatile reagents". experimental part. p. 10930 - 10940. Retrieved 2010/02/28.