1-Methyl-2-hydroxy-2-phenylethanesulfonamide

Base Information

• Chemical Name: 1-Methyl-2-hydroxy-2-phenylethanesulfonamide
• CAS No.: 129502-42-7
• Molecular Formula: C₉H₁₃NO₃S
• Molecular Weight: 215.273
• Mol file: 129502-42-7.mol

Synonyms:1-Methyl-2-hydroxy-2-phenylethanesulfonamide

Chemical Property of 1-Methyl-2-hydroxy-2-phenylethanesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Methyl-2-hydroxy-2-phenylethanesulfonamide

There total 2 articles about 1-Methyl-2-hydroxy-2-phenylethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Camphor N-<(1-methyl-2-hydroxy-2-phenylethyl)sulfonyl>imine → 1-Methyl-2-hydroxy-2-phenylethanesulfonamide (129502-42-7)

Guidance literature:

With hydrogenchloride; In ethanol; for 8h; Heating;

DOI:10.1021/jo00070a026

Reference yield: 96.0%

1-Hydroxy-1-phenyl-propane-2-sulfonic acid [1,7,7-trimethyl-bicyclo[2.2.1]hept-(2E)-ylidene]-amide (150849-98-2) → 1-Methyl-2-hydroxy-2-phenylethanesulfonamide (129502-42-7)

Guidance literature:

With hydrogenchloride; In ethanol; Heating;

DOI:10.1016/S0040-4039(00)88845-0

upstream raw materials:

1-Hydroxy-1-phenyl-propane-2-sulfonic acid [1,7,7-trimethyl-bicyclo[2.2.1]hept-(2E)-ylidene]-amide

Refernces

• 1、 Davis, Franklin A.,Zhou, Ping,Lal, G. Sankar. "A NEW SYNTHESIS OF α-FUNCTIONALIZED UNSUBSTITUTED SULFONAMIDES". . p. 1653 - 1656. Retrieved 2007/10/02.