Technology Process of Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester
There total 10 articles about Benzoic acid (E)-6-(2,2-dimethyl-6-methylene-cyclohexyl)-4-methyl-2-oxo-hex-3-enyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent
2: 94 percent / Red-Al, H+ / H2O
3: 97 percent / Bu4NF, DMAP
4: PCC
With
dmap; tetrabutyl ammonium fluoride; hydrogen cation; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate;
In
water;
DOI:10.1021/jo9610568
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 98 percent / DMSO, ClCOCOCl, Et3N
2: 100 percent
3: 94 percent / Red-Al, H+ / H2O
4: 97 percent / Bu4NF, DMAP
5: PCC
With
dmap; oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen cation; dimethyl sulfoxide; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate;
In
water;
DOI:10.1021/jo9610568
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 71 percent / TiCl4, Zn
2: 98 percent / LiAlH4
3: 96 percent / DMSO, ClCOCOCl, Et3N
4: 100 percent
5: 98 percent / DMSO, ClCOCOCl, Et3N
6: 100 percent
7: 94 percent / Red-Al, H+ / H2O
8: 97 percent / Bu4NF, DMAP
9: PCC
With
dmap; lithium aluminium tetrahydride; oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen cation; titanium tetrachloride; dimethyl sulfoxide; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; pyridinium chlorochromate; zinc;
In
water;
DOI:10.1021/jo9610568