3-chloro-1-undecenylthio benzene

Base Information

• Chemical Name: 3-chloro-1-undecenylthio benzene
• CAS No.: 198982-64-8
• Molecular Formula: C₁₇H₂₅ClS
• Molecular Weight: 296.904
• Mol file: 198982-64-8.mol

Synonyms:3-chloro-1-undecenylthio benzene

Chemical Property of 3-chloro-1-undecenylthio benzene

Chemical Property:

Purity/Quality:

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Technology Process of 3-chloro-1-undecenylthio benzene

There total 2 articles about 3-chloro-1-undecenylthio benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-phenylthio-2-undecene (198982-51-3) → 3-chloro-1-undecenylthio benzene (198982-64-8)

Guidance literature:

With sulfuryl dichloride; In tetrachloromethane; at 0 ℃; for 1h; Yield given;

DOI:10.1080/00397919708005915

Reference yield:

Undec-2-ynylsulfanyl-benzene (153940-37-5) → 3-chloro-1-undecenylthio benzene (198982-64-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 76 percent / diisobutyl aluminum hydride / hexane; diethyl ether / 2 h / Heating

2: sulfuryl chloride / CCl₄ / 1 h / 0 °C

With sulfuryl dichloride; diisobutylaluminium hydride; In tetrachloromethane; diethyl ether; hexane;

DOI:10.1080/00397919708005915

Reference yield: 42.0%

3-chloro-1-undecenylthio benzene (198982-64-8) → 2-undecenal (53448-07-0,71277-05-9,2463-77-6)

Guidance literature:

With water; copper(II) oxide; copper dichloride; In acetone; for 1h; Heating;

DOI:10.1080/00397919708005915

upstream raw materials:

1-phenylthio-2-undecene

Undec-2-ynylsulfanyl-benzene

Downstream raw materials:

2-undecenal

Refernces