Technology Process of C49H73FN4O16Si2
There total 9 articles about C49H73FN4O16Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 2,6-lutidine / CH2Cl2 / 6 h / 0 °C
2: Et3N / dioxane / 18 h / 25 °C
3: aq. LiOH / 2-methyl-propan-2-ol / 18 h / 25 °C
4: 79 percent / NaHCO3; HATU / tetrahydrofuran / 48 h / 0 °C
5: 81 percent / CrO3; aq. H2SO4 / acetone / 2 h / 0 °C
With
2,6-dimethylpyridine; chromium(VI) oxide; lithium hydroxide; sulfuric acid; sodium hydrogencarbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; acetone; tert-butyl alcohol;
DOI:10.1021/ja039795a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N / dioxane / 18 h / 25 °C
2: aq. LiOH / 2-methyl-propan-2-ol / 18 h / 25 °C
3: 79 percent / NaHCO3; HATU / tetrahydrofuran / 48 h / 0 °C
4: 81 percent / CrO3; aq. H2SO4 / acetone / 2 h / 0 °C
With
chromium(VI) oxide; lithium hydroxide; sulfuric acid; sodium hydrogencarbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; 1,4-dioxane; acetone; tert-butyl alcohol;
DOI:10.1021/ja039795a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 2,6-lutidine / CH2Cl2 / 6 h / 0 °C
2: Et3N / dioxane / 18 h / 25 °C
3: aq. LiOH / 2-methyl-propan-2-ol / 18 h / 25 °C
4: 79 percent / NaHCO3; HATU / tetrahydrofuran / 48 h / 0 °C
5: 81 percent / CrO3; aq. H2SO4 / acetone / 2 h / 0 °C
With
2,6-dimethylpyridine; chromium(VI) oxide; lithium hydroxide; sulfuric acid; sodium hydrogencarbonate; triethylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; acetone; tert-butyl alcohol;
DOI:10.1021/ja039795a