Technology Process of C38H57N7O7
There total 31 articles about C38H57N7O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
dichloromethane;
at 20 ℃;
for 72h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 2 h / 20 °C
2.1: palladium 10% on activated carbon; hydrogen / methanol; water; acetic acid / 18 h / 20 °C / 760.05 Torr
3.1: dichloromethane / 1 h / 0 - 20 °C
4.1: 4-methyl-morpholine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / dichloromethane / 20 °C
5.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / -12 - -10 °C
5.2: 18 h / 0 - 20 °C
With
4-methyl-morpholine; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; sulfur trioxide pyridine complex; triethylamine;
In
methanol; dichloromethane; water; acetic acid; dimethyl sulfoxide;
DOI:10.1021/jo502829j
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 20 - 80 °C
1.2: 1 h
1.3: DOWEX50wx8 / pH 7
2.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C
2.2: 48 h
3.1: bis(trichloromethyl) carbonate; 4-methyl-morpholine / dichloromethane / 3.08 h / -78 - -30 °C
4.1: dichloromethane / 72 h / 20 °C
With
4-methyl-morpholine; bis(trichloromethyl) carbonate; Dess-Martin periodane;
In
dichloromethane;
![(3aS,6aR)-1,3a,4,5,6,6a-hexahydrocyclopenta[c]pyrrole](/Databaselist/images/loading.webp)
