4-hydroxy-3-nitrobenzyl bromide

Base Information Edit

Chemical Name:4-hydroxy-3-nitrobenzyl bromide
CAS No.:177179-94-1
Molecular Formula:C₇H₆BrNO₃
Molecular Weight:232.034
Hs Code.:
Mol file:177179-94-1.mol

Synonyms:4-hydroxy-3-nitrobenzyl bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-hydroxy-3-nitrobenzyl bromide Edit

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Technology Process of 4-hydroxy-3-nitrobenzyl bromide

There total 3 articles about 4-hydroxy-3-nitrobenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 41833-13-0
4-hydroxymethyl-2-nitrophenol

: 177179-94-1
4-hydroxy-3-nitrobenzyl bromide

Guidance literature:: With phosphorus tribromide; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/acs.jmedchem.7b01438

Reference yield:

: 3011-34-5
4-hydroxy-3-nitrobenzaldehyde

: 177179-94-1
4-hydroxy-3-nitrobenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / ethanol / 3 h / 0 - 20 °C

2: phosphorus tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; phosphorus tribromide; In ethanol; dichloromethane;
DOI:10.1021/acs.jmedchem.7b01438