C₁₄H₁₃F₃N₂O₅

Base Information

• Chemical Name: C₁₄H₁₃F₃N₂O₅
• CAS No.: 1256257-81-4
• Molecular Formula: C₁₄H₁₃F₃N₂O₅
• Molecular Weight: 346.263
• Mol file: 1256257-81-4.mol

Synonyms:C₁₄H₁₃F₃N₂O₅

Chemical Property of C₁₄H₁₃F₃N₂O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of C₁₄H₁₃F₃N₂O₅

There total 1 articles about C₁₄H₁₃F₃N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H20N2O6 (1256257-80-3) + trifluoroacetic anhydride (407-25-0) → C14H13F3N2O5 (1256257-81-4)

Guidance literature:

C₂₀H₂₀N₂O₆; With pyridine; at 50 ℃; for 12h;

trifluoroacetic anhydride; With pyridine; at 20 ℃; for 48h;

DOI:10.1002/ejoc.201000695

Reference yield: 99.0%

C14H13F3N2O5 (1256257-81-4) → (R)-4-benzyloxycarbonylamino-4,5-dihydro-2(3H)-furanone (118399-28-3)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.201000695

upstream raw materials:

C₂₀H₂₀N₂O₆

trifluoroacetic anhydride

Downstream raw materials:

(R)-4-benzyloxycarbonylamino-4,5-dihydro-2(3H)-furanone

Refernces