C₃₈H₅₄O₈

Base Information

• Chemical Name: C₃₈H₅₄O₈
• CAS No.: 930302-47-9
• Molecular Formula: C₃₈H₅₄O₈
• Molecular Weight: 638.842
• Mol file: 930302-47-9.mol

Synonyms:C₃₈H₅₄O₈

Chemical Property of C₃₈H₅₄O₈

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₈H₅₄O₈

There total 8 articles about C₃₈H₅₄O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

trans,trans-4,4'-bicyclohexyl-bis{4-[6-(benzyloxy)hexan-1-oxy]benzoate} (930302-45-7) → C38H54O8 (930302-47-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran;

DOI:10.1016/j.tetlet.2006.12.094

Reference yield:

ethyl p-(6-benzyloxyhexan-1-oxy)benzoate (945608-49-1) → C38H54O8 (930302-47-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: aq. potassium hydroxide / ethane-1,2-diol / 7 h / Heating

2.1: oxalyl chloride; N,N-dimethylformamide / toluene

2.2: 43 percent / pyridine / toluene

3.1: 96 percent / hydrogen / Pd/C / tetrahydrofuran

With potassium hydroxide; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; ethylene glycol; toluene;

DOI:10.1016/j.tetlet.2006.12.094

Reference yield:

p-(6-benzyloxyhexan-1-oxy)benzoic acid (223268-35-7) → C38H54O8 (930302-47-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: oxalyl chloride; N,N-dimethylformamide / toluene

1.2: 43 percent / pyridine / toluene

2.1: 96 percent / hydrogen / Pd/C / tetrahydrofuran

With oxalyl dichloride; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; toluene;

DOI:10.1016/j.tetlet.2006.12.094

upstream raw materials:

trans,trans-4,4'-bicyclohexyl-bis{4-[6-(benzyloxy)hexan-1-oxy]benzoate}

6-(benzyloxy)hexyl benzenesulfonate

ethyl p-(6-benzyloxyhexan-1-oxy)benzoate

p-(6-benzyloxyhexan-1-oxy)benzoic acid

Refernces