Technology Process of 4-(4-cyclohexyl-1H-1,2,3-triazol-1-yl)-2,2-dimethyl-3,4-dihyro-2H-benzo[g]chromene-5,10-dione
There total 4 articles about 4-(4-cyclohexyl-1H-1,2,3-triazol-1-yl)-2,2-dimethyl-3,4-dihyro-2H-benzo[g]chromene-5,10-dione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
dichloromethane; water;
at 20 ℃;
DOI:10.1016/j.ejmech.2013.02.038
- Guidance literature:
-
Multi-step reaction with 4 steps
1: hydrogenchloride; acetic acid / acetic acid
2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane
3: sodium azide / dichloromethane / 24 h / 20 °C
4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 20 °C
With
hydrogenchloride; N-Bromosuccinimide; sodium azide; copper(ll) sulfate pentahydrate; acetic acid; sodium L-ascorbate; dibenzoyl peroxide;
In
tetrachloromethane; dichloromethane; water; acetic acid;
DOI:10.1016/j.ejmech.2013.02.038
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane
2: sodium azide / dichloromethane / 24 h / 20 °C
3: copper(ll) sulfate pentahydrate; sodium L-ascorbate / dichloromethane; water / 20 °C
With
N-Bromosuccinimide; sodium azide; copper(ll) sulfate pentahydrate; sodium L-ascorbate; dibenzoyl peroxide;
In
tetrachloromethane; dichloromethane; water;
DOI:10.1016/j.ejmech.2013.02.038