Technology Process of C19H30O3
There total 5 articles about C19H30O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane;
at -78 ℃;
for 1.5h;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 °C
1.2: 18.5 h / 0 - 20 °C
2.1: Dess-Martin periodane / dichloromethane / 20 °C / Cooling with ice
3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 19 h / 0 - 20 °C
4.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 1.5 h / -78 °C
With
sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: thionyl chloride / diethyl ether / 5 h
2.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 °C
2.2: 18.5 h / 0 - 20 °C
3.1: Dess-Martin periodane / dichloromethane / 20 °C / Cooling with ice
4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 19 h / 0 - 20 °C
5.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 1.5 h / -78 °C
With
thionyl chloride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride;
In
tetrahydrofuran; diethyl ether; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;
DOI:10.1021/ol3017676