mer-hydrido[[(butoxycarbonyl)methyl]cyano](butyl cyanoacetate)tris(triphenylphosphine)ruthenium(II)

Base Information

• Chemical Name: mer-hydrido[[(butoxycarbonyl)methyl]cyano](butyl cyanoacetate)tris(triphenylphosphine)ruthenium(II)
• CAS No.: 173593-97-0
• Molecular Formula: C₆₈H₆₇N₂O₄P₃Ru
• Molecular Weight: 1170.28
• Mol file: 173593-97-0.mol

Synonyms:mer-hydrido[[(butoxycarbonyl)methyl]cyano](butyl cyanoacetate)tris(triphenylphosphine)ruthenium(II)

Chemical Property of mer-hydrido[[(butoxycarbonyl)methyl]cyano](butyl cyanoacetate)tris(triphenylphosphine)ruthenium(II)

Chemical Property:

Purity/Quality:

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Technology Process of mer-hydrido[[(butoxycarbonyl)methyl]cyano](butyl cyanoacetate)tris(triphenylphosphine)ruthenium(II)

There total 1 articles about mer-hydrido[[(butoxycarbonyl)methyl]cyano](butyl cyanoacetate)tris(triphenylphosphine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

RuH*C2H4*2P(C6H5)3*P(C6H5)2(C6H4)=RuH(C2H4)(P(C6H5)3)2(P(C6H5)2C6H4) + cyanoacetic acid butyl ester (5459-58-5) → mer-hydrido[[(butoxycarbonyl)methyl]cyano](butyl cyanoacetate)tris(triphenylphosphine)ruthenium(II) (173593-97-0)

Guidance literature:

In tetrahydrofuran; byproducts: C2H4; room temp., 6 h; washing (hexane), recrystallization (THF/hexane); elem. anal.;

DOI:10.1021/ja00155a008

upstream raw materials:

cyanoacetic acid butyl ester

Refernces