toluene-4-sulfonic acid hepta-3,4-dienyl ester

Base Information

• Chemical Name: toluene-4-sulfonic acid hepta-3,4-dienyl ester
• CAS No.: 24767-75-7
• Molecular Formula: C₁₄H₁₈O₃S
• Molecular Weight: 266.361
• Mol file: 24767-75-7.mol

Synonyms:toluene-4-sulfonic acid hepta-3,4-dienyl ester

Chemical Property of toluene-4-sulfonic acid hepta-3,4-dienyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of toluene-4-sulfonic acid hepta-3,4-dienyl ester

There total 2 articles about toluene-4-sulfonic acid hepta-3,4-dienyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluenesulfonyl chloride (98-59-9) + 3,4-heptadien-1-ol (5567-51-1) → toluene-4-sulfonic acid hepta-3,4-dienyl ester (24767-75-7)

Guidance literature:

With pyridine;

DOI:10.1021/ja01045a042

Reference yield:

NaCC(n-C3H7) (58534-80-8) → toluene-4-sulfonic acid hepta-3,4-dienyl ester (24767-75-7)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) , (ii) LiAlH₄

2: Py

With pyridine;

DOI:10.1021/ja01045a042

Reference yield:

toluene-4-sulfonic acid hepta-3,4-dienyl ester (24767-75-7) → 1,3,5-heptatriene (2196-23-8)

Guidance literature:

With sodium acetate; acetic anhydride; In acetic acid;

DOI:10.1021/ja01045a042

upstream raw materials:

p-toluenesulfonyl chloride

3,4-heptadien-1-ol

NaCC(n-C₃H₇)

Downstream raw materials:

1,3,5-heptatriene

1-cyclopropyl-1-butanone

6-propyl-2,3,4,5-tetrahydropyridine

(Z)-2-but-1-enyl-pyrrolidine

Refernces