Technology Process of Naphtho[1,2-d]thiazol-2(1H)-one, hydrazone (9CI)
There total 4 articles about Naphtho[1,2-d]thiazol-2(1H)-one, hydrazone (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrochloride; hydrazine hydrate;
In
ethylene glycol;
at 140 ℃;
for 4h;
DOI:10.1002/ardp.19853180320
- Guidance literature:
-
With
hydrazine hydrate;
In
tetrahydrofuran; propan-1-ol;
at 80 ℃;
for 4h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 8 h / 25 °C / Inert atmosphere
2: hydrazine hydrate / tetrahydrofuran; propan-1-ol / 4 h / 80 °C / Inert atmosphere
With
hydrazine hydrate; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; propan-1-ol; dichloromethane;