Technology Process of BISMUTH MOLYBDATE(VI)
There total 6 articles about BISMUTH MOLYBDATE(VI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
HNO3; ammonium hydroxide;
In
water;
add. Bi(NO3)3*5H2O to 15.6M HNO3; dissolved in water; (NH4)6Mo7O24 dissolved in water; pH=2(HNO3); at 25°C mixing for 40 min at pH=2.00+/-0.07(NH4OH); aged for 30 min; filtration; calcination at 400°C for 2 h;
DOI:10.1016/0021-9517(91)90169-5
- Guidance literature:
-
With
HNO3;
In
ethylene glycol;
Mo complex dispersed in diethylene glycol, heated to 120°C, a soln. of HNO3 added, heated for 5 h to 170°C, allowed to cool to room temp., dried at 400°C for 1 h, annealed at 700°C for 12 h; not isolated, obtained as a mixt.;
DOI:10.1021/ic061198c
- Guidance literature:
-
With
ammonium hydroxide;
In
not given;
Addn. of a soln. of Bi(NO3)3*5H2O to a soln. of {NH4}6Mo7O24*4H2O, pH 7-9 (maintained by addn. of NH4OH).; Evapn., ppt. is heat treated at 450°C for 8 h, purity checked by powder X-ray diffraction and Raman spectroscopy.;
DOI:10.1021/j100321a045
