3-Propinyl-2'-phenylethylsulfid

Base Information

• Chemical Name: 3-Propinyl-2'-phenylethylsulfid
• CAS No.: 25558-00-3
• Molecular Formula: C₁₁H₁₂S
• Molecular Weight: 176.282
• Mol file: 25558-00-3.mol

Synonyms:3-Propinyl-2'-phenylethylsulfid

Chemical Property of 3-Propinyl-2'-phenylethylsulfid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 3-Propinyl-2'-phenylethylsulfid

There total 1 articles about 3-Propinyl-2'-phenylethylsulfid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

propargyl bromide (106-96-7) + sodium 2-phenylethanethiolate → 3-Propinyl-2'-phenylethylsulfid (25558-00-3)

Guidance literature:

In methanol;

DOI:10.1021/jo00910a008

Reference yield: 90.0%

3-Propinyl-2'-phenylethylsulfid (25558-00-3) → 2-mercaptophenylethane (4410-99-5)

Guidance literature:

With rubidium hydroxide; 2,6-di-tert-butyl-4-methyl-phenol; 1-hydroxy-4-isothiocyano-2,2,6,6-tetramethylpiperidine; In dimethyl sulfoxide; for 20h; Irradiation;

Reference yield:

3-Propinyl-2'-phenylethylsulfid (25558-00-3) → 1-(2-Phenylethylsulfonyl)-propin (25558-04-7)

Guidance literature:

Multi-step reaction with 2 steps

1: KOH / tetrahydrofuran

2: MCPBA

With potassium hydroxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran;

DOI:10.1021/jo00910a008

upstream raw materials:

propargyl bromide

Downstream raw materials:

1-(2-Phenylethylsulfonyl)-propin

2-mercaptophenylethane