Technology Process of 4-(tert-butoxy)-2,6-dimethylphenol
There total 7 articles about 4-(tert-butoxy)-2,6-dimethylphenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
at 20 ℃;
for 21h;
Inert atmosphere;
DOI:10.1002/anie.201310491
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sulfuric acid / 1.7 h / 20 °C / Inert atmosphere
2: sodium dithionite; sodium hydroxide / water; ethanol / 0.67 h / 20 °C / Inert atmosphere
3: magnesium(II) perchlorate / dichloromethane / 40 °C / Inert atmosphere
4: potassium carbonate / methanol / 21 h / 20 °C / Inert atmosphere
With
sodium dithionite; magnesium(II) perchlorate; sulfuric acid; potassium carbonate; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water;
DOI:10.1002/anie.201310491
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium dithionite; sodium hydroxide / water; ethanol / 0.67 h / 20 °C / Inert atmosphere
2: magnesium(II) perchlorate / dichloromethane / 40 °C / Inert atmosphere
3: potassium carbonate / methanol / 21 h / 20 °C / Inert atmosphere
With
sodium dithionite; magnesium(II) perchlorate; potassium carbonate; sodium hydroxide;
In
methanol; ethanol; dichloromethane; water;
DOI:10.1002/anie.201310491
