Hydroxylamine,O-(3-phenoxypropyl)-, hydrochloride (1:1)

Base Information

• Chemical Name: Hydroxylamine,O-(3-phenoxypropyl)-, hydrochloride (1:1)
• CAS No.: 15269-73-5
• Molecular Formula: C₉H₁₃NO₂*ClH
• Molecular Weight: 203.669
• Mol file: 15269-73-5.mol

Synonyms:Hydroxylamine,O-(3-phenoxypropyl)-, hydrochloride (8CI,9CI)

Chemical Property of Hydroxylamine,O-(3-phenoxypropyl)-, hydrochloride (1:1)

Chemical Property:

• Melting Point: 118-120 °C
• PSA: 44.48000
• LogP: 2.84810

Purity/Quality:

97% ^*data from raw suppliers

O-(3-PHENOXY-PROPYL)-HYDROXYLAMINE HYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydroxylamine,O-(3-phenoxypropyl)-, hydrochloride (1:1)

There total 3 articles about Hydroxylamine,O-(3-phenoxypropyl)-, hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(3-phenoxy-propoxy)-acetamide (1025841-61-5) → 3-phenoxy-propyl-hydroxylamine monohydrochloride (15269-73-5)

Guidance literature:

With hydrogenchloride; In methanol; for 15h;

DOI:10.1021/jm010089z

Reference yield:

phenol (108-95-2,27073-41-2) → 3-phenoxy-propyl-hydroxylamine monohydrochloride (15269-73-5)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH; tetrabutylammonium hydrogen sulfate / 31 h / 80 - 85 °C / pH 14

2: 2-methoxy-ethanol / 15 h / 60 °C

3: conc. HCl / methanol / 15 h

With hydrogenchloride; sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; In methanol; 2-methoxy-ethanol;

DOI:10.1021/jm010089z

Reference yield:

3-phenoxypropyl bromide (588-63-6) → 3-phenoxy-propyl-hydroxylamine monohydrochloride (15269-73-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 2-methoxy-ethanol / 15 h / 60 °C

2: conc. HCl / methanol / 15 h

With hydrogenchloride; In methanol; 2-methoxy-ethanol;

DOI:10.1021/jm010089z

upstream raw materials:

N-(3-phenoxy-propoxy)-acetamide

3-phenoxypropyl bromide

phenol

Refernces