2,5-bis(hydroxymethyl)-3-octylthiophene

Base Information

• Chemical Name: 2,5-bis(hydroxymethyl)-3-octylthiophene
• CAS No.: 1256466-05-3
• Molecular Formula: C₁₄H₂₄O₂S
• Molecular Weight: 256.409
• Mol file: 1256466-05-3.mol

Synonyms:2,5-bis(hydroxymethyl)-3-octylthiophene

Chemical Property of 2,5-bis(hydroxymethyl)-3-octylthiophene

Chemical Property:

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Technology Process of 2,5-bis(hydroxymethyl)-3-octylthiophene

There total 1 articles about 2,5-bis(hydroxymethyl)-3-octylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-octylthiophene (65016-62-8,104934-51-2) → 2,5-bis(hydroxymethyl)-3-octylthiophene (1256466-05-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 72 h / 0 °C / Darkness

2.1: n-butyllithium / tetrahydrofuran; hexane / -78 °C / Inert atmosphere

2.2: 12 h / -78 - 20 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

With N-Bromosuccinimide; lithium aluminium tetrahydride; n-butyllithium; In tetrahydrofuran; hexane; N,N-dimethyl-formamide;

DOI:10.1021/ma102101e

upstream raw materials:

3-octylthiophene

Refernces