Technology Process of tert-butyl 2-[2-[(tert-butoxycarbonyl)amino]ethyl]phenylcarbamate
There total 4 articles about tert-butyl 2-[2-[(tert-butoxycarbonyl)amino]ethyl]phenylcarbamate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Cyclohexanethiol; 10-phenyl-10H-phenothiazine; sodium formate;
In
water; dimethyl sulfoxide;
at 23 ℃;
for 16h;
regioselective reaction;
Irradiation;
Inert atmosphere;
Sealed tube;
Cooling;
DOI:10.1021/jacs.9b01077
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium hydroxide / water; tetrahydrofuran / 50 °C
2: sodium formate; 10-phenyl-10H-phenothiazine; Cyclohexanethiol / dimethyl sulfoxide; water / 16 h / 23 °C / Irradiation; Inert atmosphere; Sealed tube; Cooling
With
Cyclohexanethiol; 10-phenyl-10H-phenothiazine; sodium formate; lithium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/jacs.9b01077
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; dmap / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: lithium hydroxide / water; tetrahydrofuran / 50 °C
3: sodium formate; 10-phenyl-10H-phenothiazine; Cyclohexanethiol / dimethyl sulfoxide; water / 16 h / 23 °C / Irradiation; Inert atmosphere; Sealed tube; Cooling
With
dmap; Cyclohexanethiol; 10-phenyl-10H-phenothiazine; sodium formate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/jacs.9b01077