4-(2-diazoacetyl)-2-methoxyphenyl acetate

Base Information

• Chemical Name: 4-(2-diazoacetyl)-2-methoxyphenyl acetate
• CAS No.: 74162-07-5
• Molecular Formula: C₁₁H₁₀N₂O₄
• Molecular Weight: 234.211
• Mol file: 74162-07-5.mol

Synonyms:4-(2-diazoacetyl)-2-methoxyphenyl acetate

Chemical Property of 4-(2-diazoacetyl)-2-methoxyphenyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(2-diazoacetyl)-2-methoxyphenyl acetate

There total 3 articles about 4-(2-diazoacetyl)-2-methoxyphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methoxy-4-acetoxybenzoyl chloride (56681-66-4) → 4-(2-diazoacetyl)-2-methoxyphenyl acetate (74162-07-5)

Guidance literature:

With diazomethane; In diethyl ether; at -5 - 0 ℃;

DOI:10.1039/c3pp50305d

Reference yield:

4-acetoxy-3-methoxybenzoic acid (10543-12-1) → 4-(2-diazoacetyl)-2-methoxyphenyl acetate (74162-07-5)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / 8 h / 80 °C / Inert atmosphere

2: diazomethane / diethyl ether / -5 - 0 °C

With diazomethane; thionyl chloride; In diethyl ether;

DOI:10.1039/c3pp50305d

Reference yield:

→ 4-(2-diazoacetyl)-2-methoxyphenyl acetate (74162-07-5)

Guidance literature:

/BRN= 2270584/;

upstream raw materials:

3-methoxy-4-acetoxybenzoyl chloride

4-acetoxy-3-methoxybenzoic acid

Downstream raw materials:

β-oxo-β-(3,4-dimethoxyphenyl)-ethanol

α,4-diacetoxy-3-methoxyacetophenone

2,4'-dihydroxy-3'-methoxyacetophenone

diethyl (2-(4-hydroxy-3-methoxyphenyl)-2-oxoethyl) phosphate

Refernces