Technology Process of C25H28O2
There total 7 articles about C25H28O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 7600.51 Torr
2.1: polyphosphoric acid / 12 h / 80 °C
3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
3.2: 4 h / -78 °C
4.1: acetic acid; sulfuric acid / 4 h / 20 °C
5.1: sodium methylate / methanol / 0.5 h / 20 °C
5.2: 4 h / 80 °C
6.1: hydrogenchloride; water / 0.5 h / 20 °C / pH 4 - 6
With
hydrogenchloride; sulfuric acid; palladium 10% on activated carbon; water; hydrogen; sodium methylate; acetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; methanol;
2.1: |Friedel-Crafts Acylation / 5.1: |Claisen-Schmidt Condensation / 5.2: |Claisen-Schmidt Condensation;
DOI:10.1016/j.ejmech.2013.01.012
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: polyphosphoric acid / 12 h / 80 °C
2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C
2.2: 4 h / -78 °C
3.1: acetic acid; sulfuric acid / 4 h / 20 °C
4.1: sodium methylate / methanol / 0.5 h / 20 °C
4.2: 4 h / 80 °C
5.1: hydrogenchloride; water / 0.5 h / 20 °C / pH 4 - 6
With
hydrogenchloride; sulfuric acid; water; sodium methylate; acetic acid; lithium diisopropyl amide;
In
tetrahydrofuran; methanol;
1.1: |Friedel-Crafts Acylation / 4.1: |Claisen-Schmidt Condensation / 4.2: |Claisen-Schmidt Condensation;
DOI:10.1016/j.ejmech.2013.01.012
