2-Pyridinecarboximidic acid, 4-methyl-, hydrazide

Base Information

• Chemical Name: 2-Pyridinecarboximidic acid, 4-methyl-, hydrazide
• CAS No.: 1007-14-3
• Molecular Formula: C₇H₁₀N₄
• Molecular Weight: 150.183
• Hs Code.: 2933399090
• Mol file: 1007-14-3.mol

Synonyms:Picolinimidicacid, 4-methyl-, hydrazide (7CI,8CI)

Chemical Property of 2-Pyridinecarboximidic acid, 4-methyl-, hydrazide

Chemical Property:

• Melting Point: 100-101 °C
• Boiling Point: 293.8±42.0 °C(Predicted)
• PKA: 7.53±0.50(Predicted)
• PSA: 77.29000
• Density: 1.26±0.1 g/cm3(Predicted)
• LogP: 1.36960

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Pyridinecarboximidic acid, 4-methyl-, hydrazide

There total 3 articles about 2-Pyridinecarboximidic acid, 4-methyl-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Cyano-4-methylpyridin (1620-76-4) → 4-Methyl-picolinimidsaeurehydrazid (1007-14-3)

Guidance literature:

With hydrazine; In ethanol;

Reference yield:

2-acetyl-4-methylpyridine (59576-26-0) → 4-Methyl-picolinimidsaeurehydrazid (1007-14-3)

Guidance literature:

Multi-step reaction with 2 steps

1: ammonia; iodine / tetrahydrofuran; water

2: hydrazine / ethanol

With ammonia; iodine; hydrazine; In tetrahydrofuran; ethanol; water;

Reference yield:

→ 4-Methyl-picolinimidsaeurehydrazid (1007-14-3)

Guidance literature:

4-Methyl-2-cyan-pyridin, 95percentig. N2H4, A. (Raumt., 2h);

DOI:10.1021/jo01014a502

upstream raw materials:

2-acetyl-4-methylpyridine

2-Cyano-4-methylpyridin

Refernces