1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride

Base Information

• Chemical Name: 1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride
• CAS No.: 1384164-83-3
• Molecular Formula: C₂₃H₃₁N₂*Cl
• Molecular Weight: 370.966
• Mol file: 1384164-83-3.mol

Synonyms:1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride

Chemical Property of 1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride

There total 2 articles about 1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1-butylbenzimidazole (4886-30-0) + 2,3,4,5,6-pentamethylbenzyl chloride (484-65-1) → 1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride (1384164-83-3)

Guidance literature:

In N,N-dimethyl-formamide; at 25 - 80 ℃; for 12h; Inert atmosphere;

DOI:10.1016/j.inoche.2012.04.033

Reference yield:

1-(2,3,4,5,6-pentamethylbenzyl)-1H-benzo[d]imidazole + n-Butyl chloride (109-69-3) → 1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride (1384164-83-3)

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 36h; Inert atmosphere;

DOI:10.1016/j.molstruc.2019.127668

Reference yield: 71.0%

pyridine (110-86-1) + 1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazolium chloride (1384164-83-3) + palladium dichloride → Dichloro-[1-(2,3,4,5,6-pentamethylbenzyl)-3-(n-butyl)-benzimidazole-2-ylidene]-(pyridine)-palladium(II)

Guidance literature:

With potassium carbonate; at 80 ℃; for 16h;

DOI:10.1016/j.molstruc.2019.127668

upstream raw materials:

1-butylbenzimidazole

2,3,4,5,6-pentamethylbenzyl chloride

n-Butyl chloride

Refernces

• 1、 Günal, Selami,Kalo?lu, Nazan,?zdemir, Ilknur,Demir, Serpil,?zdemir, Ismail. "Novel benzimidazolium salts and their silver complexes: Synthesis and antibacterial properties". . p. 142 - 146. Retrieved 2012.