Technology Process of C62H58N8O3PS(1+)
There total 5 articles about C62H58N8O3PS(1+) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide;
In
dichloromethane;
for 10h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere
1.2: 16 h / 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 20 °C
3.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere
3.2: 16 h / 20 °C / Inert atmosphere
With
benzotriazol-1-ol; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1039/c2cc31077e
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: acetonitrile / 16 h / 80 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide / 18 h / 90 °C / Inert atmosphere
3.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere
3.2: 16 h / 20 °C / Inert atmosphere
4.1: trifluoroacetic acid / dichloromethane / 20 °C
5.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C / Inert atmosphere
5.2: 16 h / 20 °C / Inert atmosphere
With
benzotriazol-1-ol; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/c2cc31077e