4'-chloro-7-dimethylaminoheptanophenone

Base Information

• Chemical Name: 4'-chloro-7-dimethylaminoheptanophenone
• CAS No.: 76852-63-6
• Molecular Formula: C₁₅H₂₂ClNO
• Molecular Weight: 267.799
• Mol file: 76852-63-6.mol

Synonyms:4'-chloro-7-dimethylaminoheptanophenone

Chemical Property of 4'-chloro-7-dimethylaminoheptanophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4'-chloro-7-dimethylaminoheptanophenone

There total 3 articles about 4'-chloro-7-dimethylaminoheptanophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

4',7-dichloroheptanophenone (76852-66-9) + dimethyl amine (124-40-3) → 4'-chloro-7-dimethylaminoheptanophenone (76852-63-6)

Guidance literature:

With sodium iodide; In butanone; for 16h; Heating;

Reference yield:

7-chloroheptanenitrile (22819-91-6) → 4'-chloro-7-dimethylaminoheptanophenone (76852-63-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 56 percent / NaI / butan-2-one / 16 h / Heating

With sodium iodide; In butanone;

Reference yield:

(4-chlorphenyl)magnesium bromide (873-77-8) → 4'-chloro-7-dimethylaminoheptanophenone (76852-63-6)

Guidance literature:

Multi-step reaction with 2 steps

2: 56 percent / NaI / butan-2-one / 16 h / Heating

With sodium iodide; In butanone;

upstream raw materials:

4',7-dichloroheptanophenone

dimethyl amine

7-chloroheptanenitrile

(4-chlorphenyl)magnesium bromide

Downstream raw materials:

1-(4-Chloro-phenyl)-7-dimethylamino-heptan-1-one O-{2-[4-(2-hydroxy-ethyl)-piperazin-1-yl]-ethyl}-oxime

1-(4-Chloro-phenyl)-7-dimethylamino-heptan-1-one O-[2-(1-oxo-1λ⁴-thiomorpholin-4-yl)-ethyl]-oxime

1-(4-Chloro-phenyl)-7-dimethylamino-heptan-1-one O-(2-thiomorpholin-4-yl-ethyl)-oxime

1-(4-Chloro-phenyl)-7-dimethylamino-heptan-1-one O-(2-amino-propyl)-oxime

Refernces