3-(3,4-dihydroxyphenyl)propanoic acid propyl ester

Base Information

• Chemical Name: 3-(3,4-dihydroxyphenyl)propanoic acid propyl ester
• CAS No.: 90522-64-8
• Molecular Formula: C₁₂H₁₆O₄
• Molecular Weight: 224.257
• Mol file: 90522-64-8.mol

Synonyms:3-(3,4-dihydroxyphenyl)propanoic acid propyl ester

Chemical Property of 3-(3,4-dihydroxyphenyl)propanoic acid propyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(3,4-dihydroxyphenyl)propanoic acid propyl ester

There total 4 articles about 3-(3,4-dihydroxyphenyl)propanoic acid propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-(4-hydroxyphenyl)propionic acid propyl ester (83281-52-1) → 3-(3,4-dihydroxyphenyl)propanoic acid propyl ester (90522-64-8)

Guidance literature:

With Agaricus bisporus; oxygen; In aq. phosphate buffer; dichloromethane; at 25 ℃; for 24h; pH=7; Reagent/catalyst;

DOI:10.1016/j.bmc.2013.10.026

Reference yield:

4-hydroxyphenylpropionic acid (501-97-3) → 3-(3,4-dihydroxyphenyl)propanoic acid propyl ester (90522-64-8)

Guidance literature:

Multi-step reaction with 2 steps

1: chloro-trimethyl-silane / 24 h / 25 °C

2: Agaricus bisporus; oxygen / aq. phosphate buffer; dichloromethane / 24 h / 25 °C / pH 7

With chloro-trimethyl-silane; Agaricus bisporus; oxygen; In aq. phosphate buffer; dichloromethane;

DOI:10.1016/j.bmc.2013.10.026

Reference yield:

propan-1-ol (71-23-8) + dihydrocaffeic acid (1078-61-1) → 3-(3,4-dihydroxyphenyl)propanoic acid propyl ester (90522-64-8)

Guidance literature:

upstream raw materials:

propan-1-ol

dihydrocaffeic acid

4-hydroxyphenylpropionic acid

3-(4-hydroxyphenyl)propionic acid propyl ester

Refernces

• 1、 Bozzini, Tiziana,Botta, Giorgia,Delfino, Michela,Onofri, Silvano,Saladino, Raffaele,Amatore, Donatella,Sgarbanti, Rossella,Nencioni, Lucia,Palamara, Anna Teresa. "Tyrosinase and Layer-by-Layer supported tyrosinases in the synthesis of lipophilic catechols with antiinfluenza activity". . p. 7699 - 7708. Retrieved 2014/01/06.