Technology Process of 9-BROMO-9-BORABICYCLO[3.3.1]NONANE
There total 12 articles about 9-BROMO-9-BORABICYCLO[3.3.1]NONANE which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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In
1,2,5-trimethyl-benzene;
byproducts: (Br2B2Se3); from a mixture of BBr3 and (C8H14B)2Se in mesitylene a solid is precipitated (composed B2Br2Se3), the solvent is removed and oily C8H14BBr is obtained; for by-product: elem. anal., MS, mp = 325°C (dec.);
- Guidance literature:
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In
toluene;
dropping BBr3 to soln. of bis-9-borabicyclo(3,3,1)nonane at 80-120°C, stirring at 100°C for 30 min; evapn.;