5-oxo(4-nitrobenzoyl)-23-oxonemadectin

Base Information

• Chemical Name: 5-oxo(4-nitrobenzoyl)-23-oxonemadectin
• CAS No.: 133120-37-3
• Molecular Formula: C₄₃H₅₃NO₁₁
• Molecular Weight: 759.894
• Mol file: 133120-37-3.mol

Synonyms:5-oxo(4-nitrobenzoyl)-23-oxonemadectin

Chemical Property of 5-oxo(4-nitrobenzoyl)-23-oxonemadectin

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 5-oxo(4-nitrobenzoyl)-23-oxonemadectin

There total 4 articles about 5-oxo(4-nitrobenzoyl)-23-oxonemadectin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

5-oxo(4-nitrobenzoyl)-2,3-methoxime nimoxectine → 5-oxo(4-nitrobenzoyl)-23-oxonemadectin (133120-37-3)

Guidance literature:

With hydrogenchloride; In 1,3-dioxane; water; at 50 ℃; for 10h;

Reference yield: 88.0%

→ 5-oxo(4-nitrobenzoyl)-23-oxonemadectin (133120-37-3)

Guidance literature:

Reference yield:

C43H55NO11 → 5-oxo(4-nitrobenzoyl)-23-oxonemadectin (133120-37-3)

Guidance literature:

With Dess-Martin periodane; triethylamine; In dichloromethane; at 25 ℃; Reagent/catalyst; Solvent;

upstream raw materials:

4-nitro-benzoyl chloride

Downstream raw materials:

nemadectin α

Refernces

• 1、 -. "A process for preparing high-content loni mork sandbank method". Paragraph 0050-0054. . Retrieved 2017/08/26.