ethyl 4,4-dichlorocyclohexanecarboxylate

Base Information

• Chemical Name: ethyl 4,4-dichlorocyclohexanecarboxylate
• CAS No.: 444578-35-2
• Molecular Formula: C₉H₁₄Cl₂O₂
• Molecular Weight: 225.115
• Mol file: 444578-35-2.mol

Synonyms:ethyl 4,4-dichlorocyclohexanecarboxylate

Chemical Property of ethyl 4,4-dichlorocyclohexanecarboxylate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Ethyl4,4-dichlorocyclohexanecarboxylate 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ethyl 4,4-dichlorocyclohexanecarboxylate

There total 2 articles about ethyl 4,4-dichlorocyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 4-oxocyclohexane-1-carboxylate (17159-79-4) → ethyl 4,4-dichlorocyclohexanecarboxylate (444578-35-2) + 4-chloro-cyclohex-3-enecarboxylic acid ethyl ester (253276-02-7)

Guidance literature:

With phosphorus pentachloride; In toluene; at 0 - 10 ℃; for 0.666667h;

Reference yield:

ethyl 4-oxocyclohexane-1-carboxylate (17159-79-4) → ethyl 4,4-dichlorocyclohexanecarboxylate (444578-35-2) + ethyl-chlorohexanoate

Guidance literature:

With phosphorus pentachloride; at 0 ℃;

Reference yield: 25.0%

ethyl 4,4-dichlorocyclohexanecarboxylate (444578-35-2) + ethyl-chlorohexanoate → ethyl 4,4-difluorocyclohexane-1-carboxylate (178312-47-5)

Guidance literature:

With hydrogen fluoride; at 20 ℃; Product distribution / selectivity;

upstream raw materials:

ethyl 4-oxocyclohexane-1-carboxylate

Downstream raw materials:

ethyl 4,4-difluorocyclohexane-1-carboxylate

Refernces

• 1、 -. "PROCESS FOR PRODUCING FLUORINE COMPOUND". Page/Page column 7. . Retrieved 2008/06/13.