Technology Process of C66H61N7O5P2
There total 10 articles about C66H61N7O5P2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 78 percent / diethyl phosphorocyanidate, Et3N / dimethylformamide / 120 h / 20 - 23 °C
2: 82 percent / ammonium formate / 10percent Pd/C / methanol / 1 h / Ambient temperature
3: 27 percent / (i-Pr)2NEt / dimethylformamide / 25 h / 65 °C
4: N,N-dimethyl-acetamide / 120 h / 20 - 23 °C
With
diethyl cyanophosphonate; ammonium formate; triethylamine; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
methanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 78 percent / diethyl phosphorocyanidate, Et3N / dimethylformamide / 120 h / 20 - 23 °C
2: 82 percent / ammonium formate / 10percent Pd/C / methanol / 1 h / Ambient temperature
3: 27 percent / (i-Pr)2NEt / dimethylformamide / 25 h / 65 °C
4: N,N-dimethyl-acetamide / 120 h / 20 - 23 °C
With
diethyl cyanophosphonate; ammonium formate; triethylamine; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
methanol; N,N-dimethyl acetamide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 63 percent / diethyl phosphorocyanidate, N-methylmorpholine / dimethylformamide / 120 h / 20 - 23 °C
2: 88 percent / H2 / 10percent Pd/C / dioxane / Ambient temperature
3: 27 percent / (i-Pr)2NEt / dimethylformamide / 25 h / 65 °C
4: N,N-dimethyl-acetamide / 120 h / 20 - 23 °C
With
4-methyl-morpholine; diethyl cyanophosphonate; hydrogen; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
1,4-dioxane; N,N-dimethyl acetamide; N,N-dimethyl-formamide;