phenylmethane dithiol

Base Information

• Chemical Name: phenylmethane dithiol
• CAS No.: 78872-76-1
• Molecular Formula: C₇H₈S₂
• Molecular Weight: 156.273
• Mol file: 78872-76-1.mol

Synonyms:phenylmethane dithiol

Chemical Property of phenylmethane dithiol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of phenylmethane dithiol

There total 4 articles about phenylmethane dithiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

1,3-dimethylimidazolidine-2-thione (13461-16-0) + benzyl bromide (100-39-0) → 1,3-dimethyl-2-imidazolidinone (80-73-9) + phenylmethane dithiol (78872-76-1)

Guidance literature:

1,3-dimethylimidazolidine-2-thione; benzyl bromide; In water; at 100 ℃; for 2h; Inert atmosphere;

With thiourea hydrochloride; sodium hydroxide; In water; toluene; at 60 ℃; for 1h;

Reference yield:

hydrogen sulfide (7783-06-4) + benzaldehyde (100-52-7) → dibenzyl disulphide (150-60-7) + phenylmethane dithiol (78872-76-1) + (e,e,e)-cis,cis-2,4,6-triphenyl-1,3,5-trithiane (51703-77-6)

Guidance literature:

at 50 - 80 ℃;

DOI:10.1021/ja01136a004

Reference yield:

benzaldehyde (100-52-7) → phenylmethane dithiol (78872-76-1)

Guidance literature:

With hydrogen sulfide; at 75 ℃; under 36775.4 Torr;

DOI:10.1021/ja01136a004

upstream raw materials:

benzaldehyde

hydrogen sulfide

1,3-dimethylimidazolidine-2-thione

benzyl bromide

Downstream raw materials:

(μ-α,α-toluenedithiolato)bis(tricarbonyliron)

bis-benzoylmercapto-phenyl-methane

bis-acetylsulfanyl-phenyl-methane

Refernces