C₁₈H₁₈BrNO₄

Base Information

• Chemical Name: C₁₈H₁₈BrNO₄
• CAS No.: 1266337-39-6
• Molecular Formula: C₁₈H₁₈BrNO₄
• Molecular Weight: 392.249
• Mol file: 1266337-39-6.mol

Synonyms:C₁₈H₁₈BrNO₄

Chemical Property of C₁₈H₁₈BrNO₄

Chemical Property:

Purity/Quality:

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• Pictogram(s):  
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Technology Process of C₁₈H₁₈BrNO₄

There total 1 articles about C₁₈H₁₈BrNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C8H8BrNO3 (1266337-14-7) + 3-bromo-1-(4-methoxyphenyl)propyne (173019-85-7) → C18H18BrNO4 (1266337-39-6)

Guidance literature:

With indium; ammonium chloride; In tetrahydrofuran; water; at 20 ℃; for 18h; regioselective reaction;

DOI:10.1002/ejoc.201001233

Reference yield: 56.0%

C23H21NO4 (1198184-52-9) + C18H18BrNO4 (1266337-39-6) → C41H38N2O8 (1266337-49-8)

Guidance literature:

With hydroxylamine hydrochloride; ethylamine; copper(l) chloride; In methanol; dichloromethane; water; at 0 ℃; for 18h;

DOI:10.1002/ejoc.201001233

upstream raw materials:

C₈H₈BrNO₃

3-bromo-1-(4-methoxyphenyl)propyne

Downstream raw materials:

C₄₁H₃₈N₂O₈

Refernces