p-methoxyphenyl(triphenylphosphine)gold(I)

Base Information Edit

Chemical Name:p-methoxyphenyl(triphenylphosphine)gold(I)
CAS No.:127591-24-6
Molecular Formula:C₂₅H₂₂AuOP
Molecular Weight:566.389
Hs Code.:
Mol file:127591-24-6.mol

Synonyms:p-methoxyphenyl(triphenylphosphine)gold(I)

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Chemical Property of p-methoxyphenyl(triphenylphosphine)gold(I) Edit

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Technology Process of p-methoxyphenyl(triphenylphosphine)gold(I)

There total 3 articles about p-methoxyphenyl(triphenylphosphine)gold(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 5720-07-0
4-methoxyphenylboronic acid

: 127591-24-6
p-methoxyphenyl(triphenylphosphine)gold(I)

Guidance literature:: With potassium hydroxide; In water; for 1h; Milling;
DOI:10.1039/d0gc02263b

Reference yield: 90.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 13139-86-1
4-methoxyphenyl magnesium bromide

: 127591-24-6
p-methoxyphenyl(triphenylphosphine)gold(I)

Guidance literature:: In tetrahydrofuran; 4-methoxyphenylmagnesium bromide added dropwise at -78°C to soln.of ClAuPPh3 in THF in Schlenk techniques under Ar; mixt. warmed to room temp., mixed for 16 h; treated with satd. soln. of NH4Cl, extd. with Et2O; org. layers washed with satd. soln. of NaCl, dried over MgSO4; solvents removed under vac.; crystals obtained via crystn. from CHCl3;
DOI:10.1016/j.jorganchem.2005.07.080