Technology Process of tetrabromo(1,5,9,13,17,21-hexaazacyclotetracosane)dicopper(II)
There total 1 articles about tetrabromo(1,5,9,13,17,21-hexaazacyclotetracosane)dicopper(II) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
KOH;
In
ethanol;
A soln. of anhydrous CuBr2 (abs. EtOH) is added dropwise to a neutralized (gently heating to boiling, addn. of KOH, boiling with stirring for 15 min, allowing to cool to room temp., filtn.) mixt. of {12}aneN3*3HBr and {24}aneN6*6HBr in abs. EtOH.; A bright green ppt. forms, which is intermittently removed from soln. by suction filtn., this process is continued until a dark brown ppt. appears, the combined green ppts. are recrystd. from water, elem. anal.;
