S-phenyl O-ethylxanthate

Base Information

• Chemical Name: S-phenyl O-ethylxanthate
• CAS No.: 3278-38-4
• Molecular Formula: C₉H₁₀OS₂
• Molecular Weight: 198.31
• Mol file: 3278-38-4.mol

Synonyms:S-phenyl O-ethylxanthate

Chemical Property of S-phenyl O-ethylxanthate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of S-phenyl O-ethylxanthate

There total 37 articles about S-phenyl O-ethylxanthate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

sodium O-ethyl dithiocarbonate (140-90-9) + benzenediazonium tetrafluoroborate (369-57-3) → S-phenyl O-ethylxanthate (3278-38-4)

Guidance literature:

With copper diacetate; In water; acetone; Further Variations:; effect of absence of Cu salt; Product distribution;

Reference yield: 70.0%

phenyl chlorodithioformate (16911-89-0) + ethanol (64-17-5) → S-phenyl O-ethylxanthate (3278-38-4)

Guidance literature:

With pyridine; In benzene; for 1h; Heating;

DOI:10.1039/P29880000177

Reference yield: 65.0%

potassium ethyl xanthogenate (140-89-6) + benzenediazonium tetrafluoroborate (369-57-3) → S-phenyl O-ethylxanthate (3278-38-4)

Guidance literature:

In water; acetone; at -10 - 0 ℃; for 1.5h;

upstream raw materials:

phenyl chlorodithioformate

potassium ethyl xanthogenate

aniline

ethanol

Downstream raw materials:

thiophenol

carbon oxide sulfide

diphenyl sulfide

2-ethylthiophenol

Refernces

• 1、 Grishchuk,Vlasik,Blinder,Gorbovoi,Kudrik. "Synthesis and antimicrobial properties of 1-O-alkyldithiocarbonato-1-butoxy-2-arylethanes". . p. 714 - 716. Retrieved 1996.
• 2、 Hajipour, Abdol R.,Jajarmi, Saeideh,Khorsandi, Zahra. "Copper nanoparticles supported on polyaniline-functionalized multiwall carbon nanotubes: An efficient and recyclable catalyst for synthesis of unsymmetric sulfides using potassium ethyl xanthogenate in water". . . Retrieved 2017/09/01.
• 3、 Castro, Enrique A.,Pavez, Paulina,Santos, Jose G.. "Kinetics and Mechanism of the Benzenethiolysis of O-Ethyl S-(2,4-Dinitrophenyl) and O-Ethyl S-(2,4,6-Trinitrophenyl) Dithiocarbonates and O-Methyl O-(2,4-Dinitrophenyl) Thiocarbonate". . p. 9034 - 9039. Retrieved 2007/10/03.