3-formamidobenzyl bromide

Base Information Edit

Chemical Name:3-formamidobenzyl bromide
CAS No.:122488-76-0
Molecular Formula:C₈H₈BrNO
Molecular Weight:214.062
Hs Code.:
Mol file:122488-76-0.mol

Synonyms:3-formamidobenzyl bromide

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Chemical Property of 3-formamidobenzyl bromide Edit

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Technology Process of 3-formamidobenzyl bromide

There total 2 articles about 3-formamidobenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 122488-77-1
3-formamidobenzyl alcohol

: 122488-76-0
3-formamidobenzyl bromide

Guidance literature:: With phosphorus tribromide; In tetrahydrofuran; for 0.5h;
DOI:10.1021/jm00163a032

Reference yield:

: 1877-77-6
3-aminobenzenemethanol

: 122488-76-0
3-formamidobenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / 2.) 37percent aq NH₄OH / 1.) 105 deg C, 3 d, steel bomb, 2.) methanol, RT, 5 h

2: 93 percent / PBr₃ / tetrahydrofuran / 0.5 h

With ammonium hydroxide; phosphorus tribromide; In tetrahydrofuran;
DOI:10.1021/jm00163a032