Technology Process of 4-Fluorophenyl benzyl sulfide
There total 19 articles about 4-Fluorophenyl benzyl sulfide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
4-fluoro-1-iodobenzene;
With
isopropylmagnesium chloride; lithium chloride;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
Green chemistry;
benzyl thiosulphate;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
Green chemistry;
DOI:10.1021/ol500067f
- Guidance literature:
-
With
nanolayered cobalt-molybdenum sulphide with Co/(Mo+Co) mole ratio 0.83;
In
Hexadecane; toluene;
at 180 ℃;
for 18h;
under 2625.26 Torr;
chemoselective reaction;
Inert atmosphere;
Autoclave;
DOI:10.1039/c8sc05782f
- Guidance literature:
-
benzyl chloride;
With
[2,2]bipyridinyl; copper(ll) sulfate pentahydrate; sodium thiosulfate pentahydrate;
In
methanol; water;
at 80 ℃;
for 2h;
Schlenk technique;
4-fluoroaniline;
With
tert.-butylnitrite;
In
methanol; water;
at 0 - 80 ℃;
for 4.66667h;
Schlenk technique;
DOI:10.1021/ol5009747