C₂₅H₃₀N₃O₂P

Base Information

• Chemical Name: C₂₅H₃₀N₃O₂P
• CAS No.: 1293980-14-9
• Molecular Formula: C₂₅H₃₀N₃O₂P
• Molecular Weight: 435.506
• Mol file: 1293980-14-9.mol

Synonyms:C₂₅H₃₀N₃O₂P

Chemical Property of C₂₅H₃₀N₃O₂P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₅H₃₀N₃O₂P

There total 6 articles about C₂₅H₃₀N₃O₂P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C25H31N3O2P(1+)*Cl(1-) (1293980-13-8) → C25H30N3O2P (1293980-14-9)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 5h; Inert atmosphere;

DOI:10.1016/j.tetlet.2011.01.041

Reference yield:

C25H33N3O2 (1293980-12-7) → C25H30N3O2P (1293980-14-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Hexamethylphosphorous triamide; phosphorus trichloride / acetonitrile / 0 - 20 °C / Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With potassium tert-butylate; Hexamethylphosphorous triamide; phosphorus trichloride; In tetrahydrofuran; acetonitrile;

DOI:10.1016/j.tetlet.2011.01.041

Reference yield:

C25H31N3O2 → C25H30N3O2P (1293980-14-9)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium tetrahydroborate / methanol / 10 h / 0 - 20 °C

2: Hexamethylphosphorous triamide; phosphorus trichloride / acetonitrile / 0 - 20 °C / Inert atmosphere

3: potassium tert-butylate / tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

With sodium tetrahydroborate; potassium tert-butylate; Hexamethylphosphorous triamide; phosphorus trichloride; In tetrahydrofuran; methanol; acetonitrile;

DOI:10.1016/j.tetlet.2011.01.041

upstream raw materials:

C₂₅H₃₃N₃O₂

C₂₅H₃₁N₃O₂P⁽¹⁺⁾*Cl^(1-)

C₁₇H₂₅N₃O

N²-hydroxyethyldiethylenetriamine

Downstream raw materials:

C₂₅H₃₀N₃O₃P

Refernces