Technology Process of C33H47N6O8P
There total 6 articles about C33H47N6O8P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-[((4-amino-phenyl)(methoxy)-phosphinoyl)-methyl]pentane-1,5-dioic acid di-tert-butyl ester; 2-Pivaloylamino-6-formylpteridin-4-one;
With
acetic acid;
at 20 ℃;
for 0.25h;
With
acetic acid;
at 20 ℃;
for 0.166667h;
Further stages.;
DOI:10.1021/jo0707840
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 89 percent / H2 / Pd/C / tetrahydrofuran / 24 h
2.1: acetic acid / 0.25 h / 20 °C
2.2: 71 percent / borane dimethylamine complex; acetic acid / 0.17 h / 20 °C
With
hydrogen; acetic acid;
palladium on activated charcoal;
In
tetrahydrofuran;
DOI:10.1021/jo0707840
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 57 percent / potassium tert-butoxide / tetrahydrofuran / 4 h / 0 - 20 °C
2.1: 89 percent / H2 / Pd/C / tetrahydrofuran / 24 h
3.1: acetic acid / 0.25 h / 20 °C
3.2: 71 percent / borane dimethylamine complex; acetic acid / 0.17 h / 20 °C
With
potassium tert-butylate; hydrogen; acetic acid;
palladium on activated charcoal;
In
tetrahydrofuran;
1.1: Michaelis-Becker reaction;
DOI:10.1021/jo0707840