4-dichloromethyl benzaldehyde

Base Information

• Chemical Name: 4-dichloromethyl benzaldehyde
• CAS No.: 77072-05-0
• Molecular Formula: C₈H₆Cl₂O
• Molecular Weight: 189.041
• Mol file: 77072-05-0.mol

Synonyms:4-dichloromethyl benzaldehyde

Chemical Property of 4-dichloromethyl benzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-dichloromethyl benzaldehyde

There total 1 articles about 4-dichloromethyl benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

terephthalaldehyde, (623-27-8) → 4-dichloromethyl benzaldehyde (77072-05-0) + p-bis-(dichloromethyl)benzene (7398-82-5)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; at 70 ℃; for 2h; Product distribution / selectivity;

Reference yield:

4-dichloromethyl benzaldehyde (77072-05-0) → p-bis-(dichloromethyl)benzene (7398-82-5)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; at 80 ℃; for 2h; Product distribution / selectivity;

upstream raw materials:

terephthalaldehyde,

Downstream raw materials:

p-bis-(dichloromethyl)benzene

Refernces

• 1、 -. "METHOD FOR THE PREPARATION OF ALPHA, ALPHA, ALPHA', ALPHA'-TETRACHLORO-P-XYLENE". Page/Page column 3. . Retrieved 2008/06/13.