C₁₃H₁₇IO₄

Base Information

• Chemical Name: C₁₃H₁₇IO₄
• CAS No.: 1451208-43-7
• Molecular Formula: C₁₃H₁₇IO₄
• Molecular Weight: 364.18
• Mol file: 1451208-43-7.mol

Synonyms:C₁₃H₁₇IO₄

Chemical Property of C₁₃H₁₇IO₄

Chemical Property:

Purity/Quality:

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Technology Process of C₁₃H₁₇IO₄

There total 1 articles about C₁₃H₁₇IO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

1-bromo-hexane (111-25-1) + 4-Iodo-3,5-dihydroxybenzoic Acid (76447-13-7) → C13H17IO4 (1451208-43-7)

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 70 ℃;

DOI:10.1021/ol401904n

Reference yield: 64.0%

4,4,5,5-tetramethyl-2-[7-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyren-2-yl]-1,3,2-dioxaborolane + C13H17IO4 (1451208-43-7) → C42H42O8 (1451208-44-8)

Guidance literature:

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium hydrogencarbonate; tricyclohexylphosphine; In tetrahydrofuran; water; at 120 ℃; for 36h; Inert atmosphere;

DOI:10.1021/ol401904n

upstream raw materials:

1-bromo-hexane

4-Iodo-3,5-dihydroxybenzoic Acid

Downstream raw materials:

C₄₂H₄₂O₈

Refernces